Development and validation of UV spectroscopy method for the determination of posaconazole in bulk and formulation (Record no. 20349)

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003 - CONTROL NUMBER IDENTIFIER
control field OSt
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20231218144313.0
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fixed length control field 231218b xxu||||| |||| 00| 0 eng d
040 ## - CATALOGING SOURCE
Original cataloging agency AIKTC-KRRC
Transcribing agency AIKTC-KRRC
100 ## - MAIN ENTRY--PERSONAL NAME
9 (RLIN) 22455
Author Patil, Shivprasad
245 ## - TITLE STATEMENT
Title Development and validation of UV spectroscopy method for the determination of posaconazole in bulk and formulation
250 ## - EDITION STATEMENT
Volume, Issue number Vol.13(3), Jul-Sep
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Raipur
Name of publisher, distributor, etc. Asian Pharma Press
Year 2023
300 ## - PHYSICAL DESCRIPTION
Pagination 171-174p.
520 ## - SUMMARY, ETC.
Summary, etc. The present study was undertaken to develop a spectrophotometric method for the determination of Posaconazole (PCZ) in pharmaceutical dosage forms. This paper describes a simple, rapid, accurate, and precise UV-spectrophotometric method for the assay of PCZin bulk and marketed dosage forms. The validation of the developed method was carried out according to ICH guidelines concerning linearity, precision, accuracy, specificity, the limit of detection, and the limit of quantification. The diluent is aqueous methanol. Calibration curves were obtained in the concentration range of 04-20µg/ml for PCZ and with good correlation coefficients (R2=0.9981). The precisions of the new method for the drug were less than the maximum allowable limit (%RSD < 2.0) specified by the ICH. Therefore, the method was found to be accurate, reproducible, and sensitive for the analysis of PCZ in pharmaceutical dosage forms.
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
9 (RLIN) 4639
Topical term or geographic name entry element PHARMACEUTICS
700 ## - ADDED ENTRY--PERSONAL NAME
9 (RLIN) 10521
Co-Author Kshirsagar, Ajay
773 0# - HOST ITEM ENTRY
International Standard Serial Number 2231-5667
Title Asian journal of pharmaceutical analysis
Place, publisher, and date of publication Raipur A & V Publications
856 ## - ELECTRONIC LOCATION AND ACCESS
URL https://ajpaonline.com/AbstractView.aspx?PID=2023-13-3-3
Link text Click here
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme
Koha item type Articles Abstract Database
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Permanent Location Current Location Shelving location Date acquired Barcode Date last seen Price effective from Koha item type
          School of Pharmacy School of Pharmacy Archieval Section 2023-12-18 2023-1723 2023-12-18 2023-12-18 Articles Abstract Database
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