Rapid RP-HPLC quantification and stress degradation studies on alogliptin, saxagliptin, metformin in pharmaceutical dosage formulation (Record no. 21988)

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005 - DATE AND TIME OF LATEST TRANSACTION
control field 20241223143937.0
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040 ## - CATALOGING SOURCE
Original cataloging agency AIKTC-KRRC
Transcribing agency AIKTC-KRRC
100 ## - MAIN ENTRY--PERSONAL NAME
9 (RLIN) 24911
Author Vipin Prakash, G.
245 ## - TITLE STATEMENT
Title Rapid RP-HPLC quantification and stress degradation studies on alogliptin, saxagliptin, metformin in pharmaceutical dosage formulation
250 ## - EDITION STATEMENT
Volume, Issue number Vol.14(1), Jan-Mar
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Raipur
Name of publisher, distributor, etc. Asian Pharma Press
Year 2024
300 ## - PHYSICAL DESCRIPTION
Pagination 11-16p.
520 ## - SUMMARY, ETC.
Summary, etc. A Fast and simple isocratic method of stability indicating RP-HPLC technique was established for determination of Alogliptin, Saxagliptin and Metformin in pharmaceutical dosage forms. The proposed method is suitable for multicomponent analysis of commercially existing combinations in market. An LC separation of these drugs were achieved with Inertsil ODS C18 (4.6 x 250mm, 5mm) using potassium dihydrogen phosphate adjusted to pH 3: acetonitrile (85:15%V/V) in isocratic mode at 1mL min-1, at ambient temperature and detection at 280 nm. These drugs were exposed to forced degradation studies in altered stress conditions. The proposed method was found to be precise, stability indicating as no interfering peaks were noticed. Robustness studies and assay of the dosage forms were established within the limit of ICH guidelines.
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
9 (RLIN) 4639
Topical term or geographic name entry element PHARMACEUTICS
700 ## - ADDED ENTRY--PERSONAL NAME
9 (RLIN) 24652
Co-Author Suresh, A. Jerad
773 0# - HOST ITEM ENTRY
International Standard Serial Number 2231-5667
Place, publisher, and date of publication Raipur A & V Publications
Title Asian journal of pharmaceutical analysis
856 ## - ELECTRONIC LOCATION AND ACCESS
URL https://ajpaonline.com/AbstractView.aspx?PID=2024-14-1-3
Link text Click here
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Source of classification or shelving scheme
Koha item type Articles Abstract Database
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Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Permanent Location Current Location Shelving location Date acquired Barcode Date last seen Price effective from Koha item type
          School of Pharmacy School of Pharmacy Archieval Section 2024-12-23 2024-1622 2024-12-23 2024-12-23 Articles Abstract Database
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