000 -LEADER |
fixed length control field |
a |
003 - CONTROL NUMBER IDENTIFIER |
control field |
OSt |
005 - DATE AND TIME OF LATEST TRANSACTION |
control field |
20190315101521.0 |
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
fixed length control field |
190312b xxu||||| |||| 00| 0 eng d |
040 ## - CATALOGING SOURCE |
Original cataloging agency |
AIKTC-KRRC |
Transcribing agency |
AIKTC-KRRC |
100 ## - MAIN ENTRY--PERSONAL NAME |
9 (RLIN) |
8004 |
Author |
Yan, Hui |
245 ## - TITLE STATEMENT |
Title |
Study on rapid non-destructive detection of eugenol in caryophylli flos by NIR spectroscopy and partial least square |
250 ## - EDITION STATEMENT |
Volume, Issue number |
Vol. 80(6), November-December |
260 ## - PUBLICATION, DISTRIBUTION, ETC. |
Place of publication, distribution, etc. |
Mumbai |
Year |
2018 |
Name of publisher, distributor, etc. |
Indian Journal of Pharmaceutical Science |
300 ## - PHYSICAL DESCRIPTION |
Pagination |
1136-1142 |
520 ## - SUMMARY, ETC. |
Summary, etc. |
A method for rapid non-destructive detection of eugenol in caryophylli flos was developed with near-infrared spectroscopy and chemometrics. One hundred and three samples were collected, and gas chromatography with internal standard was used to determine the reference value of eugenol in caryophylli flos. Near-infrared spectra were recorded from their powders and pretreated with standard normal variate and 1st derivative, and then a model was built with the chemometrics method, partial least square. Outliers of samples were detected. When 6 factors were adopted in a model, the performance was found to be the best. For prediction set, the slope was 0.9461, the offset was 0.3008, R-square was 0.9388, root mean square error of prediction was 0.6987 %, bias was -0.2815 % and residual prediction deviation was 5.89. The statistical analysis showed the predicted results were consistent with the reference values. It is feasible that near-infrared spectroscopy could be used to rapidly and accurately detect the main active content, eugenol in caryophylli flos as a method of quality control. |
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
9 (RLIN) |
4639 |
Topical term or geographic name entry element |
PHARMACEUTICS |
700 ## - ADDED ENTRY--PERSONAL NAME |
9 (RLIN) |
8005 |
Co-Author |
Liang, Mengxing |
700 ## - ADDED ENTRY--PERSONAL NAME |
9 (RLIN) |
8006 |
Co-Author |
Han, Bangxing |
773 0# - HOST ITEM ENTRY |
Title |
Indian journal of pharmaceutical sciences |
International Standard Serial Number |
0250-474X |
Place, publisher, and date of publication |
New Delhi Indian Pharmaceutical Association |
856 ## - ELECTRONIC LOCATION AND ACCESS |
URL |
http://www.ijpsonline.com/articles/a-study-on-rapid-nondestructive-detection-of-eugenol-in-caryophylli-flos-by-nir-spectroscopy-and-partial-least-square-3573.html |
Link text |
Click here |
942 ## - ADDED ENTRY ELEMENTS (KOHA) |
Source of classification or shelving scheme |
|
Koha item type |
Articles Abstract Database |