Solvent and catalyst free efficient chemoselective synthesis of 1,1-diacetate under visible light irradiation
By: Hote, Baliram S
.
Contributor(s): Siddiqui, Tabassum A. J.
Publisher: New Delhi CSIR 2022Edition: Vol.61, Nov.Description: 1184-1187p.Subject(s): GENERAL CHEMISTRYOnline resources: Click here
In:
Indian journal of chemistry (Section B)Summary: One of the synthetic intermediates is used in many organic transformations. A method for highly efficient synthesis of
1,1-diacetate (3a-j) from mixture of various substituted benzaldehydes and acetic anhydride under solvent- and catalyst free
using visible light irradiation (150 W tungsten lamp) has been developed. The main advantages of this protocol includes
shorter reaction time, eco-friendly, mild reaction condition, easy work-up procedures, high yields of products, are the
attractive features of the present methodology. All synthesized 3a-j compounds were characterized by IR, 1H NMR and
mass spectral analysis.
| Item type | Current location | Call number | Status | Date due | Barcode | Item holds |
|---|---|---|---|---|---|---|
Articles Abstract Database
|
School of Pharmacy Archieval Section | Not for loan | 2023-0640 |
One of the synthetic intermediates is used in many organic transformations. A method for highly efficient synthesis of
1,1-diacetate (3a-j) from mixture of various substituted benzaldehydes and acetic anhydride under solvent- and catalyst free
using visible light irradiation (150 W tungsten lamp) has been developed. The main advantages of this protocol includes
shorter reaction time, eco-friendly, mild reaction condition, easy work-up procedures, high yields of products, are the
attractive features of the present methodology. All synthesized 3a-j compounds were characterized by IR, 1H NMR and
mass spectral analysis.
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