000			a
999			_c11039 _d11039
003			OSt
005			20200124092024.0
008			200124b xxu||||| |||| 00| 0 eng d
040			_aAIKTC-KRRC _cAIKTC-KRRC
100			_911896 _aMahesh Kumar, K.
245			_aConventional and microwave-assisted synthesis of coumarin-3-yl-2-oxoethyl carbamodithioates and their DNA cleavage studies
250			_aVol.58B(11), Nov
260			_aNew Delhi _bCSIR _c2019
300			_a1245-1251p.
520			_aIn situ one pot synthesis of coumarin based dithiocarbamates have been studied under conventional and microwave methods. Syntheses of coumarin based dithiocarbamates have been optimized using NaOH, K3PO4 as a base in conventional method whereas K3PO4 has given good yields in less time. The syntheses of dithiocarbamates have been carried out under microwave conditions using K3PO4 as base. The generality of microwave method has been demonstrated by synthesizing a variety of substituents in excellent yields, having short reaction time with good purity compared to those under classical conditions. All the products have been characterized by their IR, GC-MS, 1H and 13C NMR spectral data. Except 2h, 2k, 2l, all these compounds have complete DNA cleavage activity
650		0	_95009 _aGENERAL CHEMISTRY
700			_911897 _aShirahatti, Arunkumar M.
773	0		_dNew Delhi NISCAIR-CSIR 2005 _tIndian journal of chemistry (Section B)
856			_uhttp://nopr.niscair.res.in/bitstream/123456789/51462/1/IJCB%2058B%2811%29%201245-1251.pdf _yClick here
942			_2ddc _cAR