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_c17056 _d17056 |
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005 | 20220704145046.0 | ||
008 | 220704b xxu||||| |||| 00| 0 eng d | ||
040 |
_aAIKTC-KRRC _cAIKTC-KRRC |
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100 |
_917070 _aDipankar, Paula, |
||
245 | _aUltrasound mediated synthesis of aldimines from non-enolizable aldehydes at room temperature | ||
250 | _aVol.60B(12), Dec | ||
260 |
_aNew Delhi _bCSIR _c2021 |
||
300 | _a1593-1600p. | ||
520 | _aA user-friendly, energy efficient method of synthesizing N-sulfonyl aldimines at room temperature (25‒28°C) from readily available and inexpensive reagents has been developed. The method employs ultrasonication from common laboratory ultrasonic cleaner to mediate the reaction. FeCl3 as catalyst and molecular sieves as water scavenger have produced excellent yields of aldimines with short reaction time. The reaction set-up does not require inert atmosphere or anhydrous solvent thereby saving resources and time. The easily scalable method works well for the condensation of aromatic non-enolizable aldehydes and sulfonamides. | ||
650 | 0 |
_95009 _aGENERAL CHEMISTRY |
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700 |
_917074 _aKalitaa, Gitumoni |
||
773 | 0 |
_dNew Delhi NISCAIR-CSIR 2005 _tIndian journal of chemistry (Section B) |
|
856 |
_uhttp://nopr.niscpr.res.in/bitstream/123456789/58605/1/IJC%20%28Section%20B%29%2c%2060B%2c%201593-1600%20%28Dec%2c2021%29.pdf _yClick here |
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_2ddc _cAR |