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040 _aAIKTC-KRRC
_cAIKTC-KRRC
100 _97344
_aSarkar, Sumit
245 _aDetermination of structural elements of synthesized silver nano-hexagon from X-ray diffraction analysis
250 _aVol. 56(10), October
260 _aNew Delhi
_c2018
_bCSIR
300 _a765-772
520 _aSilver nano-hexagons (AgNHs) have been prepared by a chemical reduction method using poly-vinyl pyrrolidone (PVP) as a stabilizing agent. The XRD results exhibit the crystalline nature of the prepared sample, with a face centred cubic (fcc) phase. Transmission electron microscopic (TEM) results reveal that the silver nanoparticles are nearly hexagon in shape with an average size of 50 nm. Here, crystallite size has been calculated using Williamson-Hall (W-H) method, which is nearly matching with average size obtained from TEM analysis. Again, using W-H method, micro strain has been calculated, which is produced in the nano-hexagon due to dislocation of silver atoms. Further, the lattice constant of the nano-hexagons has also been estimated from the Nelson–Riley plot. Moreover, the appropriate structural parameters such as Lorentz factor, Lorentz polarization factor, dislocation density, number of atoms in a unit cell and morphological index have also been studied from the X-ray diffraction profile.
650 0 _94642
_aHumanities and Applied Sciences
700 _97345
_aDas, Ratan
773 0 _dNew Delhi CSIR-NISCAIR
_x0019-5596
_tIndian journal of pure & applied physics (IJPAP)
856 _yClick here
_uhttp://nopr.niscair.res.in/handle/123456789/45247
942 _2ddc
_cAR