Recent development in nuclear magnetic resonance as a technique for quantitative method validation (Record no. 17221)
[ view plain ]
| 000 -LEADER | |
|---|---|
| fixed length control field | a |
| 003 - CONTROL NUMBER IDENTIFIER | |
| control field | OSt |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20220729094002.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 220729b xxu||||| |||| 00| 0 eng d |
| 040 ## - CATALOGING SOURCE | |
| Original cataloging agency | AIKTC-KRRC |
| Transcribing agency | AIKTC-KRRC |
| 100 ## - MAIN ENTRY--PERSONAL NAME | |
| 9 (RLIN) | 17385 |
| Author | Sahu, R. |
| 245 ## - TITLE STATEMENT | |
| Title | Recent development in nuclear magnetic resonance as a technique for quantitative method validation |
| 250 ## - EDITION STATEMENT | |
| Volume, Issue number | Vol.83(6), Nov-Dec |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. | |
| Place of publication, distribution, etc. | Mumbai |
| Name of publisher, distributor, etc. | Indian Journal of Pharmaceutical Science |
| Year | 2021 |
| 300 ## - PHYSICAL DESCRIPTION | |
| Pagination | 1094-1106p. |
| 520 ## - SUMMARY, ETC. | |
| Summary, etc. | Nuclear magnetic resonance spectroscopy has largely given way for most important routine analysis of natural, synthetic drug candidate and related molecules. The quality control and simultaneous quantitation of different residual solvents, analytes and impurities have led analysts to further exploit nuclear magnetic resonance as a viable quantitative technique. Hence, this review focuses on the use and feasibility of this technique for quantitative method validation of drug and related compounds. Validated quantitative nuclear magnetic resonance methods were simple, robust, accurate and selective for evaluating different natural and synthetic samples using various commercially accessible compounds as internal standards. In this review numerous examples are cited giving proof of advancement in nuclear magnetic resonance technology and also for precise evaluation of molecular structures of substances in solids and liquid. Studied examples of different concurrent validation methods in the review shows that the results obtained is precise with less standard deviation when compared with other chromatography techniques. Concluding the entire review, various methodologies used for quantification and validations were reflected that proved to be a specific, selective and alternative means of method validation and it can be summarized that nuclear magnetic resonance is as reliable as the chromatography-based technique for quantitative analysis providing accuracy. |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| 9 (RLIN) | 4639 |
| Topical term or geographic name entry element | PHARMACEUTICS |
| 700 ## - ADDED ENTRY--PERSONAL NAME | |
| 9 (RLIN) | 17386 |
| Co-Author | Kumar, A. |
| 773 0# - HOST ITEM ENTRY | |
| Place, publisher, and date of publication | New Delhi |
| Title | Indian journal of pharmaceutical sciences |
| 856 ## - ELECTRONIC LOCATION AND ACCESS | |
| URL | https://www.ijpsonline.com/articles/recent-development-in-nuclear-magnetic-resonance-as-a-technique-for-quantitative-method-validation.pdf |
| Link text | Click here |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Source of classification or shelving scheme | |
| Koha item type | Articles Abstract Database |
| Withdrawn status | Lost status | Source of classification or shelving scheme | Damaged status | Not for loan | Permanent Location | Current Location | Shelving location | Date acquired | Barcode | Date last seen | Price effective from | Koha item type |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| School of Pharmacy | School of Pharmacy | Archieval Section | 2022-07-29 | 2022-1218 | 2022-07-29 | 2022-07-29 | Articles Abstract Database |